2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Base Information

Chemical Name:2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside
CAS No.:90215-03-5
Molecular Formula:C₅₆H₆₄BrNO₂₄
Molecular Weight:1215.02
Hs Code.:

2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

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Technology Process of 2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

There total 2 articles about 2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 69349-74-2
2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranosyl bromide

: 89983-48-2
2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 90215-03-5
2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; 1.) 0 deg C, 2 h, 2.) room temp., 22 h;
DOI:10.1016/0008-6215(84)85299-4

Reference yield: 41.0%

: 90215-03-5
2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Guidance literature:

Reference yield:

: 90215-03-5
2-bromoethyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-4-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

: C₄₂H₅₁NO₁₇

Guidance literature:: With hydrogen; sodium methylate; palladium on activated charcoal; for 22h; under 2016.9 Torr; Ambient temperature;
DOI:10.1016/0008-6215(84)85299-4