N--4-chlorbenzolsulfonamid

Base Information

• Chemical Name: N--4-chlorbenzolsulfonamid
• CAS No.: 13068-11-6
• Molecular Formula: C₁₁H₁₄ClNO₂S₃
• Molecular Weight: 323.889

Synonyms:

Chemical Property of N--4-chlorbenzolsulfonamid

Chemical Property:

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Technology Process of N--4-chlorbenzolsulfonamid

There total 1 articles about N--4-chlorbenzolsulfonamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 4-Chlorobenzenesulfonamide (98-64-6) → N--4-chlorbenzolsulfonamid (13068-11-6)

Guidance literature:

Multistep reaction; (i) aq. NaOH, DMF, (ii) EtHal;

Reference yield: 45.0%

N,N,N',N'-tetramethylethylendiamine (815-62-3) + N--4-chlorbenzolsulfonamid (13068-11-6) → N-<3,3-Bis(dimethylamino)-1-(ethylthio)-2-propenyliden>-4-chlorbenzolsulfonamid (99879-69-3) + N-<(Dimethylamino)(ethylmercapto)methylen>-(4-chlor)benzolsulfonamid

Guidance literature:

In diethyl ether; for 24h; Ambient temperature;

DOI:10.1007/BF00798791

Reference yield: 11.0%

N,N,N',N'-tetramethylethylendiamine (815-62-3) + N--4-chlorbenzolsulfonamid (13068-11-6) → N-<3,3-Bis(dimethylamino)-1-(ethylthio)-2-propenyliden>-4-chlorbenzolsulfonamid (99879-69-3)

Guidance literature:

In diethyl ether; for 24h; Ambient temperature;

upstream raw materials:

carbon disulfide

4-Chlorobenzenesulfonamide

Downstream raw materials:

N-<3,3-Bis(dimethylamino)-1-(ethylthio)-2-propenyliden>-4-chlorbenzolsulfonamid

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