Technology Process of β-(2,2-Dimethyltetrahydro-4-pyranyl)-β-oxopropionic Acid Anilide
There total 2 articles about β-(2,2-Dimethyltetrahydro-4-pyranyl)-β-oxopropionic Acid Anilide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / TiCl4 / pentane; diethyl ether / 1) mixed at 0 deg C, 2) reflux, 6 h.
2: 78 percent / CHCl3 / 1) room temp., 4 - 5 h, 2) reflux, 1 h.
3: 82 percent / 7percent hydrochloric acdid / 24 h / Ambient temperature
With
hydrogenchloride; titanium tetrachloride;
In
diethyl ether; chloroform; pentane;
DOI:10.1007/BF00505589
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / CHCl3 / 1) room temp., 4 - 5 h, 2) reflux, 1 h.
2: 82 percent / 7percent hydrochloric acdid / 24 h / Ambient temperature
With
hydrogenchloride;
In
chloroform;
DOI:10.1007/BF00505589
