MDL-20.093

Base Information

Chemical Name:MDL-20.093
CAS No.:92210-89-4
Molecular Formula:C₁₇H₁₉N₃O₆S
Molecular Weight:393.42
Hs Code.:

Synonyms:

Suppliers and Price of MDL-20.093

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MDL-20.093

Chemical Property:

Purity/Quality:

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Technology Process of MDL-20.093

There total 6 articles about MDL-20.093 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-N-{2-[4-(tert-Butyl-dimethyl-silanyloxy)-benzenesulfinyl]-1-hydroxymethyl-ethyl}-3-(6-methyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-acrylamide

: 92210-89-4,92210-92-9,98930-79-1,128947-79-5
MDL-20.093

Guidance literature:: With cesium fluoride; In acetonitrile; Heating;
DOI:10.1016/S0040-4039(01)81255-7

Reference yield:

: 92210-83-8
2-tert-Butoxycarbonylamino-3-(4-hydroxy-phenylsulfanyl)-propionic acid methyl ester

: 92210-89-4,92210-92-9,98930-79-1,128947-79-5
MDL-20.093

Guidance literature:: Multi-step reaction with 6 steps

1: gaseous HCl / diethyl ether

2: 49 percent / Et₃N, DCC, HOBT / dimethylformamide

3: 73 percent / imidazole / dimethylformamide

4: 93 percent / LiBH₄ / tetrahydrofuran

5: NaIO₄ / H₂O; methanol

6: CsF / acetonitrile / Heating

With 1H-imidazole; hydrogenchloride; sodium periodate; lithium borohydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; cesium fluoride; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(01)81255-7

Reference yield:

: 92210-86-1,103967-51-7
3-(4-Hydroxy-phenylsulfanyl)-2-[(E)-3-(6-methyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-acryloylamino]-propionic acid methyl ester

: 92210-89-4,92210-92-9,98930-79-1,128947-79-5
MDL-20.093

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / imidazole / dimethylformamide

2: 93 percent / LiBH₄ / tetrahydrofuran

3: NaIO₄ / H₂O; methanol

4: CsF / acetonitrile / Heating

With 1H-imidazole; sodium periodate; lithium borohydride; cesium fluoride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(01)81255-7