(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

Base Information

Chemical Name:(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester
CAS No.:142926-96-3
Molecular Formula:C₂₇H₃₉F₃O₅
Molecular Weight:500.599
Hs Code.:

Synonyms:

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Chemical Property of (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

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Technology Process of (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

There total 19 articles about (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21406-61-1
pentyltriphenylphosphonium bromide

: 142926-96-3
(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1) KOtBu / 1) ether, 45 deg C, 40 min, 2) reflux, 60 min

2: 86 percent / H₂ / 2percent Pt/C / ethyl acetate / Ambient temperature

3: 97 percent / H₂O, conc. HCl / tetrahydrofuran / 1 h / Heating

4: 4-dimethylaminopyridin, N,N'-dicyclohexylcarbodiimid / CH₂Cl₂ / 6 h / Ambient temperature

With hydrogenchloride; dmap; potassium tert-butylate; water; hydrogen; dicyclohexyl-carbodiimide; platinum on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;

Reference yield:

: 126255-98-9
(8S^*)-(+/-)-8-Hydroxy-8-<(2R^*)-5-oxo-tetrahydrofuran-2-yl>octansaeure-methylester

: 142926-96-3
(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / KOH, H₂O / methanol / 5 h / Heating

2: 80 percent / BH₃ / tetrahydrofuran / -18 deg C up to r.t., 12 h

3: 57 percent / Amberlyst 15 / methanol / 48 h / Ambient temperature

4: 1.45 g / pyridiniumchlorochromate, sodium acetate / CH₂Cl₂ / 2.5 h / Ambient temperature

5: 1) KOtBu / 1) ether, 45 deg C, 40 min, 2) reflux, 60 min

6: 86 percent / H₂ / 2percent Pt/C / ethyl acetate / Ambient temperature

7: 98 percent / H₂O, conc. HCl / tetrahydrofuran / 1 h / Heating

8: 4-dimethylaminopyridin, N,N'-dicyclohexylcarbodiimid / CH₂Cl₂ / 6 h / Ambient temperature

With hydrogenchloride; dmap; potassium hydroxide; Amberlyst 15; borane; potassium tert-butylate; water; hydrogen; sodium acetate; dicyclohexyl-carbodiimide; pyridinium chlorochromate; platinum on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;

Reference yield:

: 142925-75-5
(4R^*,5R^*)-(+/-)-5,12-Dihydroxy-4-dodecanolid

: 142926-96-3
(S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-((R)-5-oxo-tetrahydro-furan-2-yl)-tridecyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 57 percent / Amberlyst 15 / methanol / 48 h / Ambient temperature

2: 1.45 g / pyridiniumchlorochromate, sodium acetate / CH₂Cl₂ / 2.5 h / Ambient temperature

3: 1) KOtBu / 1) ether, 45 deg C, 40 min, 2) reflux, 60 min

4: 86 percent / H₂ / 2percent Pt/C / ethyl acetate / Ambient temperature

5: 98 percent / H₂O, conc. HCl / tetrahydrofuran / 1 h / Heating

6: 4-dimethylaminopyridin, N,N'-dicyclohexylcarbodiimid / CH₂Cl₂ / 6 h / Ambient temperature

With hydrogenchloride; dmap; Amberlyst 15; potassium tert-butylate; water; hydrogen; sodium acetate; dicyclohexyl-carbodiimide; pyridinium chlorochromate; platinum on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;