2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

Base Information

Chemical Name:2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile
CAS No.:102393-30-6
Molecular Formula:C₃₈H₄₄N₆
Molecular Weight:584.808
Hs Code.:

2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

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Chemical Property of 2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

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Technology Process of 2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

There total 18 articles about 2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102393-15-7
C₃₆H₅₂N₂O₄

: 102393-30-6
2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

Guidance literature:: Multi-step reaction with 6 steps

1: PhCH₂ONa / Heating

2: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

3: dimethylformamide / Heating

4: POCl₃ / CH₂Cl₂

5: NaHCO₃ / H₂O / Heating

6: cyclohexylamine / toluene / Heating

With hydrogen; sodium hydrogencarbonate; cyclohexylamine; triethylamine; sodium phenyl-methanolate; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 102393-30-6
2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

Guidance literature:: Multi-step reaction with 17 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 97 percent / ethanol / 4 h / Heating

8: 98 percent / H₂O, KOH / ethanol / Heating

9: SOCl₂ / Heating

10: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

11: B₂H₆ / tetrahydrofuran

12: PhCH₂ONa / Heating

13: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

14: dimethylformamide / Heating

15: POCl₃ / CH₂Cl₂

16: NaHCO₃ / H₂O / Heating

17: cyclohexylamine / toluene / Heating

With quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; sodium; sodium hydrogencarbonate; cyclohexylamine; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 102393-10-2
4-[4-(3-Chlorocarbonyl-propyl)-2,3,5,6-tetramethyl-phenyl]-butyryl chloride

: 102393-30-6
2-Cyano-3-{4-[4-(4-{4-[5-(2,2-dicyano-vinyl)-2,4-dimethyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3,5-dimethyl-1H-pyrrol-2-yl}-acrylonitrile

Guidance literature:: Multi-step reaction with 8 steps

1: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

2: B₂H₆ / tetrahydrofuran

3: PhCH₂ONa / Heating

4: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

5: dimethylformamide / Heating

6: POCl₃ / CH₂Cl₂

7: NaHCO₃ / H₂O / Heating

8: cyclohexylamine / toluene / Heating

With hydrogen; sodium hydrogencarbonate; cyclohexylamine; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;