(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

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Chemical Name:(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride
CAS No.:118404-12-9
Molecular Formula:C₂₃H₃₆N₂O₈S₂*ClH
Molecular Weight:569.14
Hs Code.:

(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

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Chemical Property of (S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

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Technology Process of (S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

There total 7 articles about (S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125372-56-7
(5S,6S)-1,10-dibenzyloxy-5,6-dimethoxy-3,8-dioxadecane

: 118404-12-9
(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / 10 percent Pd-C / ethanol / 2 h / Ambient temperature

2: pyridine / 0 °C

3: ethanol / 1 h / Heating

4: 5N NaOH / ethanol / 1 h / 40 °C

5: 40 percent / diethyl pyrocarbonate, Et₃N / dimethylformamide / -20 °C

6: 69 percent / diethyl pyrocarbonate, Et₃N / dimethylformamide / -20 °C

7: 2.4 N HCl / ethyl acetate / 0.5 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; hydrogen; triethylamine; diethyl dicarbonate; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.912

Reference yield:

: 125372-59-0
(+)-(5S,6S)-5,6-dimethoxy-S-(N-carbobenzyloxyglycyl)-S'-(N-carbo-tert-butoxy-L-alanyl)-1,10-dimercapto-3,8-dioxadecane

: 118404-12-9
(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.37.912

Reference yield:

: 2-[(2S,3S)-4-(2-Hydroxy-ethoxy)-2,3-dimethoxy-butoxy]-ethanol

: 118404-12-9
(S)-2-Amino-thiopropionic acid S-(2-{(2S,3S)-4-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-2,3-dimethoxy-butoxy}-ethyl) ester; hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 0 °C

2: ethanol / 1 h / Heating

3: 5N NaOH / ethanol / 1 h / 40 °C

4: 40 percent / diethyl pyrocarbonate, Et₃N / dimethylformamide / -20 °C

5: 69 percent / diethyl pyrocarbonate, Et₃N / dimethylformamide / -20 °C

6: 2.4 N HCl / ethyl acetate / 0.5 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; triethylamine; diethyl dicarbonate; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.912