Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

Base Information

Chemical Name:Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde
CAS No.:101823-12-5
Molecular Formula:C₁₀H₁₆O₃
Molecular Weight:184.235
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

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Technology Process of Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

There total 2 articles about Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101823-09-0
1-<2-(1,4-dioxenyl)>-1-cyclohexanol

: 101823-12-5
Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

Guidance literature:: With oxalic acid; silica gel; sodium hydrogencarbonate; In dichloromethane;
DOI:10.1016/S0040-4039(00)98662-3

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 101823-12-5
Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.)THF, -30 deg C; 2.) 2h, -20 deg C

2: silica gel, 5percent aqueous solution of oxalic acid, sodium hydrogenocarbonate / CH₂Cl₂

With tert.-butyl lithium; oxalic acid; silica gel; sodium hydrogencarbonate; In dichloromethane;
DOI:10.1016/S0040-4039(00)98662-3

Reference yield:

: 101823-12-5
Cyclohexylidene-(2-hydroxy-ethoxy)-acetaldehyde

: 6004-53-1
1-cyclohexyl-2-hydroxyethanone

Guidance literature:: With lithium aluminium tetrahydride; Yield given. Multistep reaction; 1.) THF, 10 min; 2.) acidic hydrolisis;
DOI:10.1016/S0040-4039(00)98662-3