8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside
CAS No.:115197-05-2
Molecular Formula:C₅₂H₇₁N₃O₁₅
Molecular Weight:978.147
Hs Code.:

8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

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Chemical Property of 8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

There total 9 articles about 8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115234-11-2
ethyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-1-thio-α-D-mannopyranoside

: 115197-05-2
8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / 0.1 M sodium methoxide / methanol / 8 h

2: 75 percent / 4 Angstroem molecular sieves, silver triflate / CH₂Cl₂ / 2 h / -70 °C

3: 4 Angstroem molecular sieves, methyl triflate / CH₂Cl₂ / 48 h

4: 0.1M sodium methoxide / methanol / 5 h / 20 °C

5: H₂S / pyridine; H₂O / 12 h / 40 °C

6: 8 h / Ambient temperature

With 4 A molecular sieve; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water;

Reference yield:

: 117107-69-4
1,2-Di-O-acetyl-4-azido-4,6-dideoxy-3-O-benzyl-α-D-mannopyranoside

: 115197-05-2
8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / boron trifluoride etherate, 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: 95 percent / 0.1 M sodium methoxide / methanol / 8 h

3: 75 percent / 4 Angstroem molecular sieves, silver triflate / CH₂Cl₂ / 2 h / -70 °C

4: 4 Angstroem molecular sieves, methyl triflate / CH₂Cl₂ / 48 h

5: 0.1M sodium methoxide / methanol / 5 h / 20 °C

6: H₂S / pyridine; H₂O / 12 h / 40 °C

7: 8 h / Ambient temperature

With 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water;

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 115197-05-2
8-methoxycarbonyloctanyl O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-O-(3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranosyl)-(1->2)-3-O-benzyl-4,6-dideoxy-4-formamido-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / 4 Angstroem molecular sieves, silver triflate / CH₂Cl₂

2: 4 Angstroem molecular sieves, methyl triflate / CH₂Cl₂ / 48 h

3: 0.1M sodium methoxide / methanol / 5 h / 20 °C

4: H₂S / pyridine; H₂O / 12 h / 40 °C

5: 8 h / Ambient temperature

With 4 A molecular sieve; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water;