C₃₄H₄₁O₈P

Base Information

Chemical Name:C₃₄H₄₁O₈P
CAS No.:130450-58-7
Molecular Formula:C₃₄H₄₁O₈P
Molecular Weight:608.668
Hs Code.:

C<sub>34</sub>H<sub>41</sub>O<sub>8</sub>P

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₁O₈P

Chemical Property:

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Technology Process of C₃₄H₄₁O₈P

There total 14 articles about C₃₄H₄₁O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128044-86-0
Methyl 4,5-O-cyclohexylidene-3-didehydro-4-epi-shikimate

: 130450-58-7
C₃₄H₄₁O₈P

Guidance literature:: Multi-step reaction with 10 steps

1: NaBH₄ / methanol; tetrahydrofuran / 1 h / 0 °C

2: 85 percent / i-Pr₂NEt / tetrahydrofuran / 12 h / 45 °C

3: 76 percent / diisobutylaluminium hydride / toluene / 3 h / -78 °C

4: 65 percent / Bu₃P / tetrahydrofuran / 0.75 h / 0 °C

5: 1.) NaIO₄, 2.) KH / 1.) 1,4-dioxane, 0 deg C, 6 h, 2.) THF, 12 h

6: 92 percent / n-Bu₄NF / hexamethylphosphoric acid triamide / 1.08 h / 105 °C

7: Na₂CO₃ / CH₂Cl₂ / 1 h / -78 °C

8: m-ClC₆H₄CO₃H, C₅H₅N / 1.) -78 deg C, 2.) 0 deg C, 0.5 h

9: 65 percent / 18-crown-6 / toluene / 0.33 h / 0 °C

10: 1.) BH₃, 2.) 3-chloroperoxybenzoic acid / 1.) THF, from 0 to 24 deg C, 2.75 h, 2.) 25 deg C, 14 h

With pyridine; sodium tetrahydroborate; sodium periodate; 18-crown-6 ether; tributylphosphine; borane; tetrabutyl ammonium fluoride; potassium hydride; diisobutylaluminium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1039/c39900000953

Reference yield:

: 35949-53-2
(-)-4,5-cyclohexylidenequinic acid lactone

: 130450-58-7
C₃₄H₄₁O₈P

Guidance literature:: Multi-step reaction with 14 steps

1: Et₃N / CH₂Cl₂ / 0.33 h / 0 °C

2: methanol; tetrahydrofuran / 0.5 h / 0 °C

3: pyridinium chlorochromate, 3 Angstroem sieves, acetic acid / 1.) 0 deg C, 4 h, 2.) 24 deg C, 1.5 h

4: Et₃N / methanol; tetrahydrofuran / 0.25 h / 24 °C

5: NaBH₄ / methanol; tetrahydrofuran / 1 h / 0 °C

6: 85 percent / i-Pr₂NEt / tetrahydrofuran / 12 h / 45 °C

7: 76 percent / diisobutylaluminium hydride / toluene / 3 h / -78 °C

8: 65 percent / Bu₃P / tetrahydrofuran / 0.75 h / 0 °C

9: 1.) NaIO₄, 2.) KH / 1.) 1,4-dioxane, 0 deg C, 6 h, 2.) THF, 12 h

10: 92 percent / n-Bu₄NF / hexamethylphosphoric acid triamide / 1.08 h / 105 °C

11: Na₂CO₃ / CH₂Cl₂ / 1 h / -78 °C

12: m-ClC₆H₄CO₃H, C₅H₅N / 1.) -78 deg C, 2.) 0 deg C, 0.5 h

13: 65 percent / 18-crown-6 / toluene / 0.33 h / 0 °C

14: 1.) BH₃, 2.) 3-chloroperoxybenzoic acid / 1.) THF, from 0 to 24 deg C, 2.75 h, 2.) 25 deg C, 14 h

With pyridine; sodium tetrahydroborate; sodium periodate; 18-crown-6 ether; tributylphosphine; 3 A molecular sieve; borane; tetrabutyl ammonium fluoride; potassium hydride; diisobutylaluminium hydride; sodium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1039/c39900000953

Reference yield:

: 123994-31-0
methyl (3S,4R,5R)-3-O-benzoyl-4,5-O-cyclohexylidene-3,4,5-trihydroxycyclohec-1-ene-1-carboxylate

: 130450-58-7
C₃₄H₄₁O₈P

Guidance literature:: Multi-step reaction with 9 steps

1: 85 percent / i-Pr₂NEt / tetrahydrofuran / 12 h / 45 °C

2: 76 percent / diisobutylaluminium hydride / toluene / 3 h / -78 °C

3: 65 percent / Bu₃P / tetrahydrofuran / 0.75 h / 0 °C

4: 1.) NaIO₄, 2.) KH / 1.) 1,4-dioxane, 0 deg C, 6 h, 2.) THF, 12 h

5: 92 percent / n-Bu₄NF / hexamethylphosphoric acid triamide / 1.08 h / 105 °C

6: Na₂CO₃ / CH₂Cl₂ / 1 h / -78 °C

7: m-ClC₆H₄CO₃H, C₅H₅N / 1.) -78 deg C, 2.) 0 deg C, 0.5 h

8: 65 percent / 18-crown-6 / toluene / 0.33 h / 0 °C

9: 1.) BH₃, 2.) 3-chloroperoxybenzoic acid / 1.) THF, from 0 to 24 deg C, 2.75 h, 2.) 25 deg C, 14 h

With pyridine; sodium periodate; 18-crown-6 ether; tributylphosphine; borane; tetrabutyl ammonium fluoride; potassium hydride; diisobutylaluminium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1039/c39900000953