(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

Base Information

Chemical Name:(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid
CAS No.:100923-27-1
Molecular Formula:C₃₈H₄₄N₆O₅
Molecular Weight:664.805
Hs Code.:

(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

There total 3 articles about (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4187-53-5,22038-87-5,42142-15-4,73069-55-3
(R)-2-methyl-p-nitrobenzylamine

: 100923-27-1
(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 1.) N,N-carbonyldiimidazole / dimethylformamide / 1.) 4 h, room temperature; 2.) 12 h, room temperature

With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;
DOI:10.1007/BF00809198

Reference yield:

: 100923-14-6
(Z)-9-tert-Butoxycarbonyl-3-ethyl-2,7-dimethyl-dipyrrin-1-one-8-propanoic acid

: 100923-27-1
(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(R)-1-amino-1-(4-nitrophenyl)-ethyl>-propionsaeureamid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 1.) N,N-carbonyldiimidazole / dimethylformamide / 1.) 4 h, room temperature; 2.) 12 h, room temperature

With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;
DOI:10.1007/BF00809198