ethyl 3--trans-propenoate

Base Information

Chemical Name:ethyl 3--trans-propenoate
CAS No.:87156-46-5
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

ethyl 3-<trans-2-(p-methoxystyryl)cyclohexen-1-yl>-trans-propenoate

Synonyms:

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Chemical Property of ethyl 3--trans-propenoate

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Technology Process of ethyl 3--trans-propenoate

There total 4 articles about ethyl 3--trans-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 823-45-0
2-(hydroxymethylene)cyclohexanone

: 87156-46-5
ethyl 3--trans-propenoate

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylsulfoxide / 12 h / 50 °C

3: 1) 10percent Pd/C / 1) cyclohexane, 2) methylcyclohexane, reflux, 6.5 h

4: 1) NaH / 1) benzene, 2) 70 degC

With sodium hydride; potassium carbonate; palladium on activated charcoal; In dimethyl sulfoxide;
DOI:10.1021/jo00171a023

Reference yield:

: 15839-23-3
2-(i-propoxymethylene)cyclohexanone

: 87156-46-5
ethyl 3--trans-propenoate

Guidance literature:: Multi-step reaction with 3 steps

2: 1) 10percent Pd/C / 1) cyclohexane, 2) methylcyclohexane, reflux, 6.5 h

3: 1) NaH / 1) benzene, 2) 70 degC

With sodium hydride; palladium on activated charcoal;
DOI:10.1021/jo00171a023

Reference yield:

: 87156-51-2
2<(p-methoxyphenyl)ethynyl>-3,4,5,6-tetrahydrobenzaldehyde

: 87156-46-5
ethyl 3--trans-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 10percent Pd/C / 1) cyclohexane, 2) methylcyclohexane, reflux, 6.5 h

2: 1) NaH / 1) benzene, 2) 70 degC

With sodium hydride; palladium on activated charcoal;
DOI:10.1021/jo00171a023