6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

Base Information

Chemical Name:6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester
CAS No.:184006-76-6
Molecular Formula:C₄₄H₅₃N₉O₇S
Molecular Weight:852.027
Hs Code.:

6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

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Chemical Property of 6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

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Technology Process of 6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

There total 1 articles about 6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77716-16-6
4-tert-butoxycarbonylamino-1-methyl-1H-pyrrole-2-carboxylic acid benzotriazol-1yl ester

: 6-({4-[(4-Amino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

: 184006-76-6
6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Yield given;

Reference yield:

: 184006-76-6
6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

: 6-{[4-({4-[(4-Amino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 184006-76-6
6-{[4-({4-[(4-tert-Butoxycarbonylamino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carbonyl}-amino)-1-methyl-1H-pyrrole-2-carbonyl]-amino}-hexanoic acid 2-(4-phenylazo-benzylsulfanyl)-ethyl ester

: C₅₇H₆₈N₁₄O₈S*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 7 steps

1: CF₃COOH / CH₂Cl₂ / 1 h / 20 °C

2: Et₃N / CH₂Cl₂ / 1.5 h / 20 °C

3: CF₃COOH / CH₂Cl₂ / 1.5 h / 20 °C

4: Et₃N / dimethylformamide / 3 h / 20 °C

5: CF₃COOH / 0.33 h / 0 °C

6: Et₃N / CH₂Cl₂ / 1 h / 20 °C

7: CH₂Cl₂

With triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;