3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

Base Information

Chemical Name:3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide
CAS No.:211674-38-3
Molecular Formula:C₃₅H₄₃N₃O₁₀
Molecular Weight:665.741
Hs Code.:

3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

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Chemical Property of 3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

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Technology Process of 3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

There total 3 articles about 3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 60835-71-4
4'-aminobenzo-15-crown-5-ether

: 87590-37-2
6-(3-Benzyloxy-4-methyl-2-nitro-benzoylamino)-hexanoyl azide

: 211674-38-3
3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

Guidance literature:: In diethyl ether; chloroform;

Reference yield:

: 60835-69-0
4'-nitrobenzo-15-crown-5

: 211674-38-3
3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / dioxane / 18 °C

2: 40 percent / diethyl ether; CHCl₃

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; chloroform;

Reference yield:

: 87590-28-1
3-Benzyloxy-N-(5-hydrazinocarbonyl-pentyl)-4-methyl-2-nitro-benzamide

: 211674-38-3
3-Benzyloxy-4-methyl-2-nitro-N-[5-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-pentyl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: HCl, NaNO₂ / aq. acetic acid

2: 40 percent / diethyl ether; CHCl₃

With hydrogenchloride; sodium nitrite; In diethyl ether; chloroform; acetic acid;