5-acetyl-7b-benzyl-7bH-cyclopentindene

Base Information

Chemical Name:5-acetyl-7b-benzyl-7bH-cyclopentindene
CAS No.:97568-02-0
Molecular Formula:C₂₀H₁₆O
Molecular Weight:272.346
Hs Code.:

5-acetyl-7b-benzyl-7bH-cyclopent<cd>indene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-acetyl-7b-benzyl-7bH-cyclopentindene

Chemical Property:

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Technology Process of 5-acetyl-7b-benzyl-7bH-cyclopentindene

There total 3 articles about 5-acetyl-7b-benzyl-7bH-cyclopentindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7b-Benzyl-2a-methoxy-6,7b-dihydro-2aH-cyclopenta[cd]indene

: 97568-02-0
5-acetyl-7b-benzyl-7bH-cyclopentindene

Guidance literature:: Multi-step reaction with 2 steps

1: PTSA / 0.5 h / Ambient temperature

2: boron trifluoride - diethyl ether / CH₂Cl₂ / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; toluene-4-sulfonic acid; In dichloromethane;

Reference yield:

: 97567-97-0,97591-72-5
(2aS,7bS)-7b-Benzyl-2a-methoxy-2a,6,7,7b-tetrahydro-2H-cyclopenta[cd]inden-2-ol

: 97568-02-0
5-acetyl-7b-benzyl-7bH-cyclopentindene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) MTPI; 2.) 10percent sodium hydroxide / 1.) HMPA, room temp., 8 h.; 2.) 1 h.

2: PTSA / 0.5 h / Ambient temperature

3: boron trifluoride - diethyl ether / CH₂Cl₂ / 3 h / Ambient temperature

With sodium hydroxide; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; In dichloromethane;

Reference yield:

: 108-24-7
acetic anhydride

: 97567-98-1
7b-benzyl-7bH-cyclopentindene

: 97568-03-1
6-acetyl-7b-benzyl-7bH-cyclopentindene

: 97568-02-0
5-acetyl-7b-benzyl-7bH-cyclopentindene

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 3h; Yield given. Yields of byproduct given; Ambient temperature;