{4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Base Information

• Chemical Name: {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester
• CAS No.: 137506-39-9
• Molecular Formula: C₆₂H₇₃N₉O₉
• Molecular Weight: 1088.32

Synonyms:

Chemical Property of {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

There total 2 articles about {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C69H80N10O12 (137506-35-5) → {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester (137506-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: DPPA, NaHCO₃ / dimethylformamide

2: H₂ / 10 percent Pd/C

With diphenyl-phosphinic acid; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)92279-2

Reference yield:

C69H78N10O11 (137506-37-7) → {4-[(2S,5S,8S,11S,14S,17R)-8-(4-Amino-butyl)-11-benzyl-14-(4-hydroxy-benzyl)-17-(1H-indol-3-ylmethyl)-5-isopropyl-10-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid 9H-fluoren-9-ylmethyl ester (137506-39-9)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1016/S0040-4039(00)92279-2

upstream raw materials:

C₆₉H₇₈N₁₀O₁₁

C₆₉H₈₀N₁₀O₁₂

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