(Z)-1-phenylsulphinyl-1,4-pentadiene

Base Information

Chemical Name:(Z)-1-phenylsulphinyl-1,4-pentadiene
CAS No.:137905-34-1
Molecular Formula:C₁₁H₁₂OS
Molecular Weight:192.282
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-phenylsulphinyl-1,4-pentadiene

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Technology Process of (Z)-1-phenylsulphinyl-1,4-pentadiene

There total 2 articles about (Z)-1-phenylsulphinyl-1,4-pentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17101-71-2
Z-β-bromovinyl phenyl sulfide

: 137905-34-1
(Z)-1-phenylsulphinyl-1,4-pentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / (1,2-bis(diphenylphosphino)ethane)nickel(II) chloride / diethyl ether / 5 h / Ambient temperature

2: 2.0 g / m-chloroperbenzoic acid / CHCl₃ / 2 h / ice-bath cooling

With 3-chloro-benzenecarboperoxoic acid; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In diethyl ether; chloroform;
DOI:10.1016/S0040-4020(01)89751-9

Reference yield:

: 129196-66-3,137905-33-0
1-phenylsulphenyl-1,4-pentadiene

: 137905-34-1
(Z)-1-phenylsulphinyl-1,4-pentadiene

: 137905-35-2
(E)-1-phenylsulphinyl-1,4-pentadiene

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; ice-bath cooling;
DOI:10.1016/S0040-4020(01)89751-9

Reference yield:

: 137905-34-1,137905-35-2
1-phenylsulphinyl-1,4-pentadiene

: 84230-76-2
trans-1-Phenylsulfinylmethyl-1,3-butadiene

Guidance literature:: With n-butyllithium; methyl iodide; Yield given. Multistep reaction; 1) THF, hexane, -78 deg C, 30 min, 2a) THF, -78 deg C, 6 h, 2b) r.t., 3 h (or with Me₃SiOOSiMe₃ instead of MeI);
DOI:10.1016/S0040-4020(01)89751-9