5-amino-3-benzyl-1,2,3-oxadiazol-3-ium chloride

Base Information

Chemical Name:5-amino-3-benzyl-1,2,3-oxadiazol-3-ium chloride
CAS No.:3441-51-8
Molecular Formula:C9H10 N3 O . Cl
Molecular Weight:211.651
Hs Code.:

Synonyms:1,2,3-Oxadiazolium,5-amino-3-(phenylmethyl)-, chloride (9CI); Sydnone imine, 3-(phenylmethyl)-,monohydrochloride; Sydnone imine, 3-benzyl-, hydrochloride (7CI); Sydnoneimine, 3-benzyl-, monohydrochloride (8CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-3-benzyl-1,2,3-oxadiazol-3-ium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-amino-3-benzyl-1,2,3-oxadiazol-3-ium chloride

There total 3 articles about 5-amino-3-benzyl-1,2,3-oxadiazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3010-05-7
benzylaminoacetonitrile

: 3441-51-8,26758-48-5
5-amino-3-benzyl-[1,2,3]oxadiazolium; chloride

Guidance literature:: benzylaminoacetonitrile; With tert.-butylnitrite; In tetrahydrofuran; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/acs.orglett.0c00600

Reference yield:

: 100-46-9
benzylamine

: 3441-51-8,26758-48-5
5-amino-3-benzyl-[1,2,3]oxadiazolium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C

2.1: tert.-butylnitrite / tetrahydrofuran / 2 h / 20 °C

2.2: 20 °C

With tert.-butylnitrite; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/acs.orglett.0c00600