2-azidophenyl 1-naphthylmethyl ketone

Base Information

Chemical Name:2-azidophenyl 1-naphthylmethyl ketone
CAS No.:80749-43-5
Molecular Formula:C₁₈H₁₃N₃O
Molecular Weight:287.321
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azidophenyl 1-naphthylmethyl ketone

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Technology Process of 2-azidophenyl 1-naphthylmethyl ketone

There total 3 articles about 2-azidophenyl 1-naphthylmethyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-20-5
2-methyl-1H-indole

: 80749-43-5
2-azidophenyl 1-naphthylmethyl ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) EtMgBr / 1.) Et₂O, 2 h, reflux; 2.) Et₂O, 30 min

2: 1.) BH₃*SMe₂, 2.) CH₃OH / 1.) THF, 0 deg C, 2 h; r.t., 2 h, 2.) THF, 1 h, reflux

3: 71 percent / O₃/O₂ / ethyl acetate / 11 h

4: 77 percent / 5M HCl / ethanol / 3 h / Heating

5: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.)H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

With hydrogenchloride; methanol; sodium azide; dimethylsulfide borane complex; ethylmagnesium bromide; oxygen; ozone; sodium nitrite; In ethanol; ethyl acetate;

Reference yield:

: 879-18-5
naphthalene-1-carbonic acid chloride

: 80749-43-5
2-azidophenyl 1-naphthylmethyl ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) EtMgBr / 1.) Et₂O, 2 h, reflux; 2.) Et₂O, 30 min

2: 1.) BH₃*SMe₂, 2.) CH₃OH / 1.) THF, 0 deg C, 2 h; r.t., 2 h, 2.) THF, 1 h, reflux

3: 71 percent / O₃/O₂ / ethyl acetate / 11 h

4: 77 percent / 5M HCl / ethanol / 3 h / Heating

5: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.)H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

With hydrogenchloride; methanol; sodium azide; dimethylsulfide borane complex; ethylmagnesium bromide; oxygen; ozone; sodium nitrite; In ethanol; ethyl acetate;

Reference yield:

: 80749-39-9
2-aminophenyl 1-naphthylmethyl ketone

: 80749-43-5
2-azidophenyl 1-naphthylmethyl ketone

Guidance literature:: With hydrogenchloride; sodium azide; sodium nitrite; Yield given. Multistep reaction; 1.)H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min;