1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

Base Information

Chemical Name:1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside
CAS No.:174019-76-2
Molecular Formula:C₂₁H₁₉FO₇
Molecular Weight:402.376
Hs Code.:

Synonyms:

Suppliers and Price of 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

There total 2 articles about 1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-24-7
acetic anhydride

: 174174-99-3
methyl 5-deoxy-5-fluoro-2,3-di-O-benzoyl-β-D-ribofuranoside

: 174019-76-2
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

Guidance literature:: With sulfuric acid; In acetic acid; 1.) 0 deg C, 1 h, 2.) room temperature, 22 h;
DOI:10.1080/15257779508010707

Reference yield:

: 151266-35-2
methyl 5-deoxy-5-fluoro-β-D-ribofuranoside

: 174019-76-2
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / Ambient temperature

2: 78 percent / H₂SO₄ / acetic acid / 1.) 0 deg C, 1 h, 2.) room temperature, 22 h

With pyridine; sulfuric acid; In acetic acid;
DOI:10.1080/15257779508010707

Reference yield:

: 174019-76-2
1-O-acetyl-2,3-di-O-benzoyl-5-deoxy-5-fluoro-β-D-ribofuranoside

: 174019-80-8
C₂₆H₂₂FN₅O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HMDS, Me₃SiCl, 2.) TMSTf / 1.) xylene, reflux, 18 h, 2.) 1,2-dichloroethane, room temperature, overnight

2: 90 percent / H₂, Et₃N / palladium on charcoal / dioxane / 24 h / Ambient temperature

3: H₂S / pyridine / 1.5 h

With chloro-trimethyl-silane; TMSTf; hydrogen sulfide; hydrogen; triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; palladium on activated charcoal; In 1,4-dioxane; pyridine;
DOI:10.1080/15257779508010707