20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Base Information

Chemical Name:20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on
CAS No.:105141-42-2
Molecular Formula:C₂₈H₃₃NO₃
Molecular Weight:431.575
Hs Code.:

20-Benzoylamino-21-hydroxy-4,9<sup>(11)</sup>,17<sup>(20)</sup>-pregnatrien-3-on

Synonyms:

Suppliers and Price of 20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

There total 8 articles about 20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 104203-29-4,104203-30-7
21-Acetoxy-20-benzoylamino-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

: 105141-42-2
20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Guidance literature:: With potassium hydrogencarbonate; In methanol; water; for 3h; Heating;

Reference yield:

: 1199-01-5,53766-22-6
2-phenylazlactone

: 105141-42-2
20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / TiCl₄, pyridine / tetrahydrofuran; CCl₄ / 1.) 0-5 deg C, 20 min.; 2.) 2 h, room temp.

2: Na/CH₃OH / methanol

3: 93 percent / sodium dihydridobis(2-methoxyethoxy)aluminate (70percent) / toluene; tetrahydrofuran / 1 h / -5 °C

4: pyridine / benzene

5: 66 percent / HgO, BF₃-Et₂O / tetrahydrofuran; H₂O / Ambient temperature

6: 69 percent / KHCO₃ / methanol; H₂O / 3 h / Heating

With pyridine; methanol; boron trifluoride diethyl etherate; sodium; titanium tetrachloride; potassium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; mercury(II) oxide; In tetrahydrofuran; methanol; tetrachloromethane; water; toluene; benzene;

Reference yield:

: 1035-69-4
androst-4,9⁽¹¹⁾-dien-3,17-dione

: 105141-42-2
20-Benzoylamino-21-hydroxy-4,9⁽¹¹⁾,17⁽²⁰⁾-pregnatrien-3-on

Guidance literature:: Multi-step reaction with 7 steps

1: 66 percent / BF₃-Et₂O / methanol / 0.25 h / Ambient temperature

2: 78 percent / TiCl₄, pyridine / tetrahydrofuran; CCl₄ / 1.) 0-5 deg C, 20 min.; 2.) 2 h, room temp.

3: Na/CH₃OH / methanol

4: 93 percent / sodium dihydridobis(2-methoxyethoxy)aluminate (70percent) / toluene; tetrahydrofuran / 1 h / -5 °C

5: pyridine / benzene

6: 66 percent / HgO, BF₃-Et₂O / tetrahydrofuran; H₂O / Ambient temperature

7: 69 percent / KHCO₃ / methanol; H₂O / 3 h / Heating

With pyridine; methanol; boron trifluoride diethyl etherate; sodium; titanium tetrachloride; potassium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; mercury(II) oxide; In tetrahydrofuran; methanol; tetrachloromethane; water; toluene; benzene;