(2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC^5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester

Base Information

• Chemical Name: (2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC^5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester
• CAS No.: 73955-80-3
• Molecular Formula: C₂₃H₂₁Cl₃N₂O₃S
• Molecular Weight: 511.856

Synonyms:

Chemical Property of (2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC^5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC^5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester

There total 4 articles about (2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC^5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

benzylidene phenylamine (538-51-2) + (2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester (51056-24-7) → (3S,8aR)-2,2,2-trichloroethyl 2,3,8,8a-tetrahydro-2,2-dimethyl-5-oxo-6,8-diphenyl-5H-thiazolo<3,2-a>pyrimidine-3-carboxylate (109706-75-4) + (3S,6'S)-2,2,2-trichloroethyl 1,3-diphenylspiro (73955-80-3,109784-81-8,109784-82-9) + C23H21Cl3N2O3S (73955-80-3,109784-81-8,109784-82-9)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 5 ℃; for 0.5h;

Reference yield: 23.0%

benzylidene phenylamine (538-51-2) + (2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester (51056-24-7) → (3S,8aR)-2,2,2-trichloroethyl 2,3,8,8a-tetrahydro-2,2-dimethyl-5-oxo-6,8-diphenyl-5H-thiazolo<3,2-a>pyrimidine-3-carboxylate (109706-75-4) + (3S,6'S)-2,2,2-trichloroethyl 1,3-diphenylspiro (73955-80-3,109784-81-8,109784-82-9) + C23H21Cl3N2O3S (73955-80-3,109784-81-8,109784-82-9)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 5 ℃; for 0.5h;

Reference yield:

benzylidene phenylamine (538-51-2) + (2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester (51056-24-7) → (2Ξ,5'R)-3',3'-dimethyl-7'-oxo-1,3ξ-diphenyl-(2rC5',5'r'H)-spiro[aziridine-2,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2'c'-carboxylic acid 2,2,2-trichloro-ethyl ester (73955-80-3,109784-81-8,109784-82-9) + (7aR)-7-anilino-2,2-dimethyl-5-oxo-6-phenyl-(7ar)-2,3,5,7a-tetrahydro-pyrrolo[2,1-b]thiazole-3c-carboxylic acid 2,2,2-trichloro-ethyl ester (73973-91-8)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 5 ℃;

upstream raw materials:

benzylidene phenylamine

(2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester

(3S,6'S)-2,2,2-trichloroethyl 1,3-diphenylspiro

Downstream raw materials:

(3S,7aR)-2,2,2-trichloroethyl-7-anilino-2,3,5,7a-tetrahydro-2,2-dimethyl-5-oxo-6-phenylpyrrolo<2,1-b>thiazole-3-carboxylate

C₂₃H₂₁Cl₃N₂O₃S

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