2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Base Information

Chemical Name:2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose
CAS No.:109898-72-8
Molecular Formula:C₃₈H₄₆N₂O₁₆
Molecular Weight:786.787
Hs Code.:

2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O-<benzyl-(2-acetamido-3,4-di-O-acetyl-2-desoxy-β-D-mannopyranosyl)uronat>-2-desoxy-β-D-glucopyranose

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Chemical Property of 2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

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Technology Process of 2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

There total 9 articles about 2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55682-57-0
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 109898-72-8
2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) silver silicate, molecular sieves 4 Angstroem / 1.) toluol, 3 h, r.t., 2.) toluol

2: 97 percent / 0.1 M NaOMe / methanol / 8 h / Ambient temperature

3: 82 percent / O₂ / Pt (Adam's-katalysator) / H₂O; propan-1-ol / 6 h / 80 °C / NaHCO₃, pH 7.5

4: 62 percent / diethyl ether; methanol / Ambient temperature

5: 86 percent / pyridine / 7 h / 0 °C

6: 100 percent / trifluoroacetic acid / 6.5 h / Ambient temperature

7: H₂S / pyridine; H₂O / 24 h / Ambient temperature

8: pyridine / 6 h / 0 °C

With pyridine; silver silicate; 4 A molecular sieve; hydrogen sulfide; oxygen; sodium methylate; trifluoroacetic acid; platinum(IV) oxide; In pyridine; methanol; propan-1-ol; diethyl ether; water;
DOI:10.1016/0008-6215(86)80006-4

Reference yield:

: 95451-83-5
1,6-Anhydro-2-azido-4-O-(2-azido-2-desoxy-β-D-mannopyranosyl)-3-O-benzyl-2-desoxy-β-D-glucopyranose

: 109898-72-8
2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / O₂ / Pt (Adam's-katalysator) / H₂O; propan-1-ol / 6 h / 80 °C / NaHCO₃, pH 7.5

2: 62 percent / diethyl ether; methanol / Ambient temperature

3: 86 percent / pyridine / 7 h / 0 °C

4: 100 percent / trifluoroacetic acid / 6.5 h / Ambient temperature

5: H₂S / pyridine; H₂O / 24 h / Ambient temperature

6: pyridine / 6 h / 0 °C

With pyridine; hydrogen sulfide; oxygen; trifluoroacetic acid; platinum(IV) oxide; In pyridine; methanol; propan-1-ol; diethyl ether; water;
DOI:10.1016/0008-6215(86)80006-4

Reference yield:

: 1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-mannopyranosyl)-β-D-glucopyranose

: 109898-72-8
2-Acetamido-1,6-di-O-acetyl-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / 0.1 M NaOMe / methanol / 8 h / Ambient temperature

2: 82 percent / O₂ / Pt (Adam's-katalysator) / H₂O; propan-1-ol / 6 h / 80 °C / NaHCO₃, pH 7.5

3: 62 percent / diethyl ether; methanol / Ambient temperature

4: 86 percent / pyridine / 7 h / 0 °C

5: 100 percent / trifluoroacetic acid / 6.5 h / Ambient temperature

6: H₂S / pyridine; H₂O / 24 h / Ambient temperature

7: pyridine / 6 h / 0 °C

With pyridine; hydrogen sulfide; oxygen; sodium methylate; trifluoroacetic acid; platinum(IV) oxide; In pyridine; methanol; propan-1-ol; diethyl ether; water;
DOI:10.1016/0008-6215(86)80006-4