C₃₃H₃₉F₃N₄O₅

Base Information

Chemical Name:C₃₃H₃₉F₃N₄O₅
CAS No.:795307-85-6
Molecular Formula:C₃₃H₃₉F₃N₄O₅
Molecular Weight:628.692
Hs Code.:

C<sub>33</sub>H<sub>39</sub>F<sub>3</sub>N<sub>4</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₃H₃₉F₃N₄O₅

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Technology Process of C₃₃H₃₉F₃N₄O₅

There total 8 articles about C₃₃H₃₉F₃N₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₄N₂O₅

: 795307-85-6
C₃₃H₃₉F₃N₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: R-alphine borane / 168 h / Neat (no solvent)

2: 5%-palladium/activated carbon; hydrogen / methanol

3: sodium cyanoborohydride / methanol

4: triethylamine / tetrahydrofuran

5: trifluoroacetic acid / dichloromethane

6: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide

7: trifluoroacetic acid / dichloromethane

With 5%-palladium/activated carbon; R-alphine borane; hydrogen; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.007

Reference yield:

: 439151-11-8
(2S,3S)-[2-(tert-butoxycarbonylamino)-3-hydroxy-hex-4-ynyl]-carbamic acid benzyl ester

: 795307-85-6
C₃₃H₃₉F₃N₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1: 5%-palladium/activated carbon; hydrogen / methanol

2: sodium cyanoborohydride / methanol

3: triethylamine / tetrahydrofuran

4: trifluoroacetic acid / dichloromethane

5: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide

6: trifluoroacetic acid / dichloromethane

With 5%-palladium/activated carbon; hydrogen; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.007

Reference yield:

: C₂₀H₃₄N₂O₃

: 795307-85-6
C₃₃H₃₉F₃N₄O₅

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran

2: trifluoroacetic acid / dichloromethane

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide

4: trifluoroacetic acid / dichloromethane

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.007