8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Base Information

• Chemical Name: 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside
• CAS No.: 106450-67-3
• Molecular Formula: C₇₆H₈₉O₂₅P
• Molecular Weight: 1433.5

Synonyms:

Chemical Property of 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Chemical Property:

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Useful:

Technology Process of 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

There total 2 articles about 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl chloride (106466-85-7) + 9-((4aR,6S,7S,8S,8aS)-7-Benzyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-nonanoic acid methyl ester (106450-66-2) → 8-methoxycarbonyloctyl-3-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (106450-67-3,106499-41-6) + 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (106450-67-3,106499-41-6)

Guidance literature:

With 4 A molecular sieve; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane;

Reference yield: 22.0%

2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl chloride (106466-85-7) + 9-((4aR,6S,7S,8S,8aS)-7-Benzyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-nonanoic acid methyl ester (106450-66-2) → 8-methoxycarbonyloctyl-3-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (106450-67-3,106499-41-6) + 8-methoxycarbonyloctyl-2-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-β-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (106450-67-3,106499-41-6)

Guidance literature:

With 4 A molecular sieve; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane;

Reference yield:

8-methoxycarbonyloctyl-3-O-<2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl>-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (106450-67-3,106499-41-6) → C48H67O25P

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

upstream raw materials:

2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-diphenylphosphoryl-α-D-mannopyranosyl chloride

9-((4aR,6S,7S,8S,8aS)-7-Benzyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-nonanoic acid methyl ester

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