diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate

Base Information

• Chemical Name: diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate
• CAS No.: 120591-51-7
• Molecular Formula: C₄₆H₆₀O₆
• Molecular Weight: 708.979

Synonyms:

Chemical Property of diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate

There total 5 articles about diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

etretinate (54350-48-0) → diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1β,2α-dicarboxylate (120591-51-7,120664-45-1,120664-46-2,120664-47-3) + diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate (120591-51-7,120664-45-1,120664-46-2,120664-47-3)

Guidance literature:

With 13,17-bis(2-carboxylatoethyl)-3,8-bis[1-hydroxyethyl]-2,7,12,18-tetramethylporphine; In ethanol; at 20 - 23 ℃; for 3h; Irradiation;

DOI:10.1016/S0040-4020(01)85884-1

Reference yield: 57.0%

etretinate (54350-48-0) → diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1β,2α-dicarboxylate (120591-51-7,120664-45-1,120664-46-2,120664-47-3) + diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate (120591-51-7,120664-45-1,120664-46-2,120664-47-3)

Guidance literature:

With 13,17-bis(2-carboxylatoethyl)-3,8-bis[1-hydroxyethyl]-2,7,12,18-tetramethylporphine; In ethanol; at 20 - 23 ℃; for 3h; Irradiation;

DOI:10.1016/S0040-4020(01)85884-1

Reference yield: 56.6%

etretinate (54350-48-0) → diethyl-6β-<(1E,3E,5Z)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatrienyl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxamide (120591-51-7,120664-45-1,120664-46-2,120664-47-3) + diethyl-6α-<(1E,3E,5Z)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatrienyl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1β,2β-dicarboxamide (120591-51-7,120664-45-1,120664-46-2,120664-47-3) + diethyl-6α-<(all-E)-6-(4-methoxy-2,3,6-trimethylphenyl)-4-methyl-1,3,5-hexatriene-yl>-5α-<(all-E)-4-(4-methoxy-2,3,6-trimethylphenyl)-2-methyl-1,3-butadienyl>-3,6-dimethyl-3-cyclohexene-1α,2α-dicarboxylate (120591-51-7,120664-45-1,120664-46-2,120664-47-3)

Guidance literature:

With 13,17-bis(2-carboxylatoethyl)-3,8-bis[1-hydroxyethyl]-2,7,12,18-tetramethylporphine; In ethanol; at 20 - 23 ℃; for 3h; Irradiation;

DOI:10.1016/S0040-4020(01)85884-1

upstream raw materials:

etretinate

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