6-benzoyl-6-methylfulvene dimethyl acetal

Base Information

Chemical Name:6-benzoyl-6-methylfulvene dimethyl acetal
CAS No.:81528-09-8
Molecular Formula:C₁₆H₁₈O₂
Molecular Weight:242.318
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-benzoyl-6-methylfulvene dimethyl acetal

Chemical Property:

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Technology Process of 6-benzoyl-6-methylfulvene dimethyl acetal

There total 1 articles about 6-benzoyl-6-methylfulvene dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57711-28-1
1,1-dimethoxy-1-phenylpropan-2-one

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 81528-09-8
6-benzoyl-6-methylfulvene dimethyl acetal

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, 0.5 h, 0 deg C, 2.) 12 h, room temp.;

Reference yield:

: 81528-09-8
6-benzoyl-6-methylfulvene dimethyl acetal

: 4-methyl-6-phenyl-2,5-dioxatricyclo<4.3.0.0^4,7>non-8-en-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 458 mg / O₂ / hexane / 16 h / Ambient temperature; Irradiation

2: 83 percent / 10percent H₂SO₄ on silica gel / CH₂Cl₂ / 13 h / Ambient temperature

3: 30 percent / acetone / 5 h / -60 °C / Irradiation

With sulfuric acid; oxygen; In hexane; dichloromethane; acetone;

Reference yield:

: 81528-09-8
6-benzoyl-6-methylfulvene dimethyl acetal

: 81528-14-5
3-benzoyl-3-methyloxepin-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 458 mg / O₂ / hexane / 16 h / Ambient temperature; Irradiation

2: 83 percent / 10percent H₂SO₄ on silica gel / CH₂Cl₂ / 13 h / Ambient temperature

With sulfuric acid; oxygen; In hexane; dichloromethane;