C₄₁H₅₈N₄O₂₄

Base Information

• Chemical Name: C₄₁H₅₈N₄O₂₄
• CAS No.: 217180-20-6
• Molecular Formula: C₄₁H₅₈N₄O₂₄
• Molecular Weight: 990.924
• Mol file: 217180-20-6.mol

Synonyms:

Chemical Property of C₄₁H₅₈N₄O₂₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₅₈N₄O₂₄

There total 6 articles about C₄₁H₅₈N₄O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C48H64N4O24 (217180-18-2) → C41H58N4O24 (217180-20-6)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/ja9819458

Reference yield:

3,4,6-tetra-O-acetyl-2-O-(2,4,6-tri-O-acetyl-3-O-carbamoyl-α-D-mannopyranosyl)-α-L-gulopyranosyl diphenylphosphate (162111-91-3) → C41H58N4O24 (217180-20-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 58 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.33 h / 0 °C

2: 1.) piperidine / 1.) 25 deg C

3: 99 percent / H₂ / 10percent Pd/C

With piperidine; trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium on activated charcoal; In dichloromethane;

DOI:10.1021/ja9819458

Reference yield:

4-[(1R,2S)-2-Benzyloxycarbonyl-2-(9H-fluoren-9-ylmethoxycarbonylamino)-1-hydroxy-ethyl]-imidazole-1-carboxylic acid 9H-fluoren-9-ylmethyl ester → C41H58N4O24 (217180-20-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 58 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.33 h / 0 °C

2: 1.) piperidine / 1.) 25 deg C

3: 99 percent / H₂ / 10percent Pd/C

With piperidine; trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium on activated charcoal; In dichloromethane;

DOI:10.1021/ja9819458

upstream raw materials:

L-erythro-N^α,N^im-di-tert-butoxycarbonyl-β-hydroxyhistidine benzyl ester

C₄₈H₆₄N₄O₂₄

N^α,N^im-bis(tert-butoxycarbonyl)-erythro-β-hydroxy-L-histidine

3,4,6-tetra-O-acetyl-2-O-(2,4,6-tri-O-acetyl-3-O-carbamoyl-α-D-mannopyranosyl)-α-L-gulopyranosyl diphenylphosphate