N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid

Base Information

Chemical Name:N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid
CAS No.:80607-01-8
Molecular Formula:C₁₅H₁₆N₄O₇
Molecular Weight:364.315
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid

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Technology Process of N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid

There total 2 articles about N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 131230-07-4
Bicyclo<2.2.1>hept-1-ylmethylketoxim-pikrat

: 80607-01-8
N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid

Guidance literature:: With ClC₄H₈Cl; at 80 ℃; Beckmann rearrangement;

Reference yield:

: 88-88-0
2,4,6-trinitrochlorobenzene

: 80607-01-8
N-Bicyclo<2.2.1>hept-1-yl-N-pikrylacetamid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / acetone / 5 h / 0 °C

2: 1,4-dichlorobutane / 74 - 86 °C / Chapman variant of the Beckmann rearrangement, ΔH*, ΔS*

With pyridine; 1,4-dichlorobutane; In acetone;