(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

Base Information

Chemical Name:(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid
CAS No.:182690-11-5
Molecular Formula:C₃₀H₃₈N₂O₉
Molecular Weight:570.64
Hs Code.:

(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

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Chemical Property of (S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

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Technology Process of (S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

There total 10 articles about (S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112635-78-6
(S)-(-)-3-(tert-butyldimethylsilyloxy)-3-phenylpropanoic acid

: 182690-11-5
(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / DCC, DMAP

2: 58 percent / TPPTS, Pd(OAc)2

3: 18 percent / DCC, DMAP

4: HF / acetonitrile

5: TPPTS, Pd(OAc)2

With dmap; palladium diacetate; hydrogen fluoride; trisodium tris(3-sulfophenyl)phosphine; dicyclohexyl-carbodiimide; In acetonitrile;
DOI:10.1016/0040-4039(96)01421-9

Reference yield:

: 182690-14-8
(S)-2-((S)-2-Methylamino-propionylamino)-propionic acid allyl ester

: 182690-11-5
(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: BOP-Cl, DIEA / CH₂Cl₂

2: K₂CO₃ / methanol; H₂O

3: 18 percent / DCC, DMAP

4: HF / acetonitrile

5: TPPTS, Pd(OAc)2

With dmap; palladium diacetate; hydrogen fluoride; trisodium tris(3-sulfophenyl)phosphine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/0040-4039(96)01421-9

Reference yield:

: (S)-3-Hydroxy-3-phenyl-propionic acid allyl ester

: 182690-11-5
(S)-2-[(S)-2-({(S)-2-[(S)-3-((S)-3-Hydroxy-3-phenyl-propionyloxy)-3-phenyl-propionyloxy]-3-methyl-butyryl}-methyl-amino)-propionylamino]-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / DCC, DMAP

2: 58 percent / TPPTS, Pd(OAc)2

3: 18 percent / DCC, DMAP

4: HF / acetonitrile

5: TPPTS, Pd(OAc)2

With dmap; palladium diacetate; hydrogen fluoride; trisodium tris(3-sulfophenyl)phosphine; dicyclohexyl-carbodiimide; In acetonitrile;
DOI:10.1016/0040-4039(96)01421-9