Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

Base Information

Chemical Name:Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)
CAS No.:289907-20-6
Molecular Formula:C₂₄H₃₈N₄Ti
Molecular Weight:430.473
Hs Code.:

Ti(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

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Technology Process of Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

There total 1 articles about Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 223130-50-5
TiCl₂(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

: 6921-34-2
benzylmagnesium chloride

: 289907-20-6
Ti(CH₂C₆H₅)2(t-BuN)(1,3,5-trimethyl-1,3,5-triazacyclohexane)

Guidance literature:: In tetrahydrofuran; diethyl ether; under Ar or N2, 1.0 M BzMgCl in Et2O was added to thf soln. of Ti-compd.Mg:Ti molar ratio was 2:1) at -50 °C in the absence of light, soln. was allowed to warm to room temp., stirred for 18 h; 1,4-dioxane was added with stirring, volatiles were removed under vac.,solid was extd. into toluene, soln. was filtered, concd., hexane was added with stirring, ppt. was filtered off, washed twice with hexane, dried in vac., elem. anal.;
DOI:10.1016/S0022-328X(00)00032-2