bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

Base Information

Chemical Name:bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine
CAS No.:93359-25-2
Molecular Formula:C₆₀H₇₄N₈O₄
Molecular Weight:971.299
Hs Code.:

Synonyms:

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Chemical Property of bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

Chemical Property:

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Technology Process of bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

There total 10 articles about bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34549-87-6
ethyl 4-butyl-3,5-dimethylpyrrole-2-carboxylate

: 93359-25-2
bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

Guidance literature:: Multi-step reaction with 9 steps

1: 67 percent / sodium / 4 h / 80 °C / 15 Torr

2: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

3: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

4: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

5: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

6: 70 percent / sodium / 4 h / 80 °C / 15 Torr

7: 60 percent / paratoluenesulfonic acid / benzene / 48 h / Heating

8: triethylamine, Pd/C, hydrogen / tetrahydrofuran / 1.67 h

9: 1.) CCl₃CO₂H, HC(OMe)3, 2.) dichloro-dicyano parabenzoquinone / 1.) CH₂Cl₂, 4 h

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; dichloro-dicyano parabenzoquinone; hydrogen; iodine; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; trimethyl orthoformate; trichloroacetic acid; In tetrahydrofuran; ethanol; water; benzene;

Reference yield:

: 1540-36-9
3-butylpentane-2,4-dione

: 93359-25-2
bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

Guidance literature:: Multi-step reaction with 10 steps

1: 1.) zinc, sodium acetate / 1.) acetic acid, 80 deg C, 40 min; 2.) acetic acid, 20 min, 95-105 deg C

2: 67 percent / sodium / 4 h / 80 °C / 15 Torr

3: 1.) sulfuryl chloride / 1.) ether, 18 h, 10-15 deg C; 2.) water

4: 70 percent / triethylamine, hydrogen, 10percent palladium on carbon / tetrahydrofuran

5: 1.) sodium bicarbonate; 2.) sodium iodide, iodine / 1.) water, 1,2-dichloroethane, 50 deg C, 5 min; 2.) reflux, 1 h

6: 88 percent / sodium iodide, hydrochloric acid / ethanol; H₂O / 1 h / Heating

7: 70 percent / sodium / 4 h / 80 °C / 15 Torr

8: 60 percent / paratoluenesulfonic acid / benzene / 48 h / Heating

9: triethylamine, Pd/C, hydrogen / tetrahydrofuran / 1.67 h

10: 1.) CCl₃CO₂H, HC(OMe)3, 2.) dichloro-dicyano parabenzoquinone / 1.) CH₂Cl₂, 4 h

With hydrogenchloride; palladium on activated charcoal; sulfuryl dichloride; dichloro-dicyano parabenzoquinone; hydrogen; iodine; sodium acetate; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; zinc; trimethyl orthoformate; trichloroacetic acid; In tetrahydrofuran; ethanol; water; benzene;

Reference yield:

: 93341-76-5
ethyl 3-butyl-4-methyl-1H-pyrrole-2-carboxylate

: 93359-25-2
bis(diacetamido-2,6 phenyl)-5,15 tetrabutyl-2,8,12,18 tetramethyl-3,7,13,17 porphyrine

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / sodium / 4 h / 80 °C / 15 Torr

2: 60 percent / paratoluenesulfonic acid / benzene / 48 h / Heating

3: triethylamine, Pd/C, hydrogen / tetrahydrofuran / 1.67 h

4: 1.) CCl₃CO₂H, HC(OMe)3, 2.) dichloro-dicyano parabenzoquinone / 1.) CH₂Cl₂, 4 h

With palladium on activated charcoal; dichloro-dicyano parabenzoquinone; hydrogen; sodium; toluene-4-sulfonic acid; triethylamine; trimethyl orthoformate; trichloroacetic acid; In tetrahydrofuran; benzene;