Technology Process of N,N-Bis(3-amino-3,3-dimethylpropyl)-4-methylbenzolsulfonamid Dihydrochlorid
There total 8 articles about N,N-Bis(3-amino-3,3-dimethylpropyl)-4-methylbenzolsulfonamid Dihydrochlorid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran;
Yield given;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 70 percent / NaI / acetone / 72 h / Heating
2: 1.) Li-diisopropylamid / 1.) THF, 0 deg C, 30 min, 2.) THF, 0 deg C, 2 h
3: 25percent KOH / ethanol / Heating
4: 57.5 mmol / DMFA, Oxyalylchlorid / benzene / 16 h / 25 °C
5: 25percent aq. NaN3 / acetone / 1 h / 0 °C
6: CCl4 / 1.67 h / Heating
7: 6 N HCl / tetrahydrofuran / Heating
With
hydrogenchloride; potassium hydroxide; sodium azide; Oxyalylchlorid; N,N-dimethyl-formamide; sodium iodide; lithium diisopropyl amide;
In
tetrahydrofuran; tetrachloromethane; ethanol; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 90 percent / Et3N / CH2Cl2 / 0.5 h / 0 °C
2: 70 percent / NaI / acetone / 72 h / Heating
3: 1.) Li-diisopropylamid / 1.) THF, 0 deg C, 30 min, 2.) THF, 0 deg C, 2 h
4: 25percent KOH / ethanol / Heating
5: 57.5 mmol / DMFA, Oxyalylchlorid / benzene / 16 h / 25 °C
6: 25percent aq. NaN3 / acetone / 1 h / 0 °C
7: CCl4 / 1.67 h / Heating
8: 6 N HCl / tetrahydrofuran / Heating
With
hydrogenchloride; potassium hydroxide; sodium azide; Oxyalylchlorid; triethylamine; N,N-dimethyl-formamide; sodium iodide; lithium diisopropyl amide;
In
tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; acetone; benzene;
