η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]

Base Information

Chemical Name:η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]
CAS No.:72659-04-2
Molecular Formula:C₁₆H₁₇FeNO₅S₂
Molecular Weight:423.294
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]

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Technology Process of η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]

There total 1 articles about η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40866-96-4
N-sulfinylmethanesulfonamide

: (η5-C5H5)Fe(CO)2CH2CH2C6H5

: 72659-04-2
η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]

Guidance literature:: In chloroform; under N2 slight excess of N-sulfinylsulfonamide in CHCl3 or CH2Cl2 added dropwise to a stirred soln. of Fe-complex in the same solvent, reaction completed within 1 h; solvent removed, residue treated with 10 % H2O in acetone to destroy excess amide, solvent evapd., residue dissolved in CHCl3, soln. dried over MgSO4, filtered, filtrate concd., cooled to 0°C;

Reference yield:

: 72659-04-2
η5-Fe(CO)2[N[S(O)CH2CH2C6H5][S(O)2CH3]]

: 72659-10-0
η5-Fe(CO)2[N[S(O)2CH2CH2C6H5][S(O)2CH3]]

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; under N2 Fe-complex treated with slight excess of m-chloroperoxybenzoicacid, soln. stirred at 25°C for 1 h; solvent removed, residue treated with MeOH and large excess of NaHCO3, slurry stirred for 1 h, excess NaHCO3 filtered off, washed with MeOH, filtrate and washed combined, solvent evapd., residue dissolved in CH2Cl2,soln. dried over MgSO4, filtered...;