Re(CO)4CH(NC₆H₄F)2

Base Information

• Chemical Name: Re(CO)4CH(NC₆H₄F)2
• CAS No.: 73169-51-4
• Molecular Formula: C₁₇H₉F₂N₂O₄Re
• Molecular Weight: 529.473

Synonyms:

Chemical Property of Re(CO)4CH(NC₆H₄F)2

Chemical Property:

Purity/Quality:

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Technology Process of Re(CO)4CH(NC₆H₄F)2

There total 2 articles about Re(CO)4CH(NC₆H₄F)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

octacarbonylbis(μ-chloro)dirhenium(I) + N,N’-bis(4-fluorophenyl)formamidine (141417-89-2,18464-36-3) → Re(CO)4CH(NC6H4F)2 (73169-51-4)

Guidance literature:

In diethyl ether; byproducts: LiCl; (N); soln. of formamidinederiv. and BuLi was stirred for 2 min, then Recomplex was added and mixt. was stirred for 2 h at room temp.; mixt. was added to hexane, ether distd. off, suspn. was filtered hot and solvent was removed; benzene soln. of residue was chromd. (alumina, benzene), first eluate was evapd. to dryness, residue washed with EtOH andrecrystd. from hexane; elem. anal.;

DOI:10.1016/S0022-328X(00)83511-1

Reference yield:

Re(CO)4CON(C6H4F)CHN(C6H4F) → Re(CO)4CH(NC6H4F)2 (73169-51-4)

Guidance literature:

In methyl cyclohexane; byproducts: CO; (N2); soln. of Re complex was refluxed until no educt was detectible byIR; filtered suspn. was concd. yielding product, identified by IR and MAS;

DOI:10.1016/S0022-328X(00)83511-1

upstream raw materials:

N,N’-bis(4-fluorophenyl)formamidine

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