((CH₃)2C₆H₃NCCH₃C₅H₃N)2C₆H₃OH

Base Information

• Chemical Name: ((CH₃)2C₆H₃NCCH₃C₅H₃N)2C₆H₃OH
• CAS No.: 959464-11-0
• Molecular Formula: C₃₆H₃₄N₄O
• Molecular Weight: 538.692
• Mol file: 959464-11-0.mol

Synonyms:

Chemical Property of ((CH₃)2C₆H₃NCCH₃C₅H₃N)2C₆H₃OH

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of ((CH₃)2C₆H₃NCCH₃C₅H₃N)2C₆H₃OH

There total 1 articles about ((CH₃)2C₆H₃NCCH₃C₅H₃N)2C₆H₃OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,6-[O=C(Me)C5H3N]2C6H3OH + 2,4-Xylidine (95-68-1) → ((CH3)2C6H3NCCH3C5H3N)2C6H3OH (959464-11-0)

Guidance literature:

With formic acid; at 160 ℃;

DOI:10.1039/b709385c

Reference yield: 29.0%

((CH3)2C6H3NCCH3C5H3N)2C6H3OH (959464-11-0) + zinc(II) chloride (7646-85-7,24359-56-6) → (2,6-[2,4-Me2C6H3N=C(Me)C5H3N]2C6H3O)Zn2(μ-Cl)Cl2

Guidance literature:

In butan-1-ol; (under N2, Schlenk); ZnCl2 and n-butanol heated to 110°C, ligand added, stirred and heated to 110°C overnight, cooled to room temp.; concd., washed with hexane;

DOI:10.1039/b709385c

upstream raw materials:

2,4-Xylidine