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Technology Process of ((CH3)2C6H3NCCH3C5H3N)2C6H3OH

((CH3)2C6H3NCCH3C5H3N)2C6H3OH

Base Information
  • Chemical Name:((CH3)2C6H3NCCH3C5H3N)2C6H3OH
  • CAS No.:959464-11-0
  • Molecular Formula:C36H34N4O
  • Molecular Weight:538.692
  • Hs Code.:
((CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NCCH<sub>3</sub>C<sub>5</sub>H<sub>3</sub>N)2C<sub>6</sub>H<sub>3</sub>OH

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Chemical Property of ((CH3)2C6H3NCCH3C5H3N)2C6H3OH
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Technology Process of ((CH3)2C6H3NCCH3C5H3N)2C6H3OH

There total 1 articles about ((CH3)2C6H3NCCH3C5H3N)2C6H3OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,6-[O=C(Me)C<sub>5</sub>H<sub>3</sub>N]2C<sub>6</sub>H<sub>3</sub>OH

2,6-[O=C(Me)C5H3N]2C6H3OH

2,4-Xylidine
95-68-1

2,4-Xylidine

((CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NCCH<sub>3</sub>C<sub>5</sub>H<sub>3</sub>N)2C<sub>6</sub>H<sub>3</sub>OH
959464-11-0

((CH3)2C6H3NCCH3C5H3N)2C6H3OH

Guidance literature:
With formic acid; at 160 ℃;
DOI:10.1039/b709385c

Reference yield: 29.0%

((CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NCCH<sub>3</sub>C<sub>5</sub>H<sub>3</sub>N)2C<sub>6</sub>H<sub>3</sub>OH
959464-11-0

((CH3)2C6H3NCCH3C5H3N)2C6H3OH

zinc(II) chloride
7646-85-7,24359-56-6

zinc(II) chloride

(2,6-[2,4-Me2C6H3N=C(Me)C5H3N]2C6H3O)Zn2(μ-Cl)Cl2

(2,6-[2,4-Me2C6H3N=C(Me)C5H3N]2C6H3O)Zn2(μ-Cl)Cl2

Guidance literature:
In butan-1-ol; (under N2, Schlenk); ZnCl2 and n-butanol heated to 110°C, ligand added, stirred and heated to 110°C overnight, cooled to room temp.; concd., washed with hexane;
DOI:10.1039/b709385c
upstream raw materials:

2,4-Xylidine

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