3--5,7-dimethoxy-1-methylcarbazole

Base Information

Chemical Name:3--5,7-dimethoxy-1-methylcarbazole
CAS No.:153616-03-6
Molecular Formula:C₂₉H₃₆N₂O₆S
Molecular Weight:540.681
Hs Code.:

3-<N-(2,2-diethoxyethyl)-N-p-tosylaminomethyl>-5,7-dimethoxy-1-methylcarbazole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--5,7-dimethoxy-1-methylcarbazole

Chemical Property:

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Technology Process of 3--5,7-dimethoxy-1-methylcarbazole

There total 6 articles about 3--5,7-dimethoxy-1-methylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 98-59-9
p-toluenesulfonyl chloride

: 153616-05-8
3-(2,2-diethoxyethylaminomethyl)-5,7-dimethoxy-1-methylcarbazole

: 40597-44-2
N-(2,2-diethoxy-ethyl)-4-methylbenzenesulfonamide

: 153616-03-6
3--5,7-dimethoxy-1-methylcarbazole

Guidance literature:: With pyridine; for 96h;

Reference yield:

: 129819-79-0
3-cyano-5,7-dimethoxy-1-methylcarbazole

: 153616-03-6
3--5,7-dimethoxy-1-methylcarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) diisobutylaluminium hydride, 2.) aq. HCl / 1) diglyme, -70 deg C - -60 deg C, 0.5 h, -60 deg C --> 20 deg C, 2 h; 2) CH₃OH, diglyme, 1.5 h

2: 99 percent / 2 h / Heating

3: 85 percent / H₂ / platinium dioxide / ethanol / 20 °C

4: 40 percent / pyridine / 96 h

With pyridine; hydrogenchloride; hydrogen; diisobutylaluminium hydride; platinum(IV) oxide; In ethanol;

Reference yield:

: 146308-30-7
N-(3',5'-dimethoxyphenyl)-4-(5,5-dimethyl-1,3-dioxan-2-yl)-2-methylaniline

: 153616-03-6
3--5,7-dimethoxy-1-methylcarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 11 percent / palladium(II) acetate / acetic acid / 2 h / Heating

2: 99 percent / 2 h / Heating

3: 85 percent / H₂ / platinium dioxide / ethanol / 20 °C

4: 40 percent / pyridine / 96 h

With pyridine; hydrogen; palladium diacetate; platinum(IV) oxide; In ethanol; acetic acid;