C₁₈H₁₉ClN₂

Base Information

Chemical Name:C₁₈H₁₉ClN₂
CAS No.:81049-95-8
Molecular Formula:C₁₈H₁₉ClN₂
Molecular Weight:298.815
Hs Code.:

C<sub>18</sub>H<sub>19</sub>ClN<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₉ClN₂

Chemical Property:

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Technology Process of C₁₈H₁₉ClN₂

There total 5 articles about C₁₈H₁₉ClN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69584-88-9
4-(2-fluorophenyl)-1-methylpiperidine-4-carbonitrile

: 81049-95-8
C₁₈H₁₉ClN₂

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / lithium triethoxyaluminum hydride, lithium aluminum hydride / 1,2-dimethoxy-ethane / 72 h / Heating

2: 56 percent / NaH / dimethylsulfoxide / 4 h / 64 - 70 °C

3: 64 percent / K₂CO₃ / CH₂Cl₂ / 2 h / Ambient temperature

4: LiAlH₄ / tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; sodium hydride; potassium carbonate; lithium triethoxyaluminum hydride; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00361a009

Reference yield:

: 81049-94-7
1-(2-chlorophenyl)-1'-cyanospiro(indoline-3,4'-piperidine)

: 81049-95-8
C₁₈H₁₉ClN₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jm00361a009

Reference yield:

: 348-51-6
1-chloro-2-fluorobenzene

: 81049-95-8
C₁₈H₁₉ClN₂

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / NaH / dimethylsulfoxide / 4 h / 64 - 70 °C

2: 64 percent / K₂CO₃ / CH₂Cl₂ / 2 h / Ambient temperature

3: LiAlH₄ / tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00361a009