1,4-bis(diphenylphosphino)-2,5-difluorobenzene

Base Information

Chemical Name:1,4-bis(diphenylphosphino)-2,5-difluorobenzene
CAS No.:176174-70-2
Molecular Formula:C₃₀H₂₂F₂P₂
Molecular Weight:482.449
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis(diphenylphosphino)-2,5-difluorobenzene

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Technology Process of 1,4-bis(diphenylphosphino)-2,5-difluorobenzene

There total 1 articles about 1,4-bis(diphenylphosphino)-2,5-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 327-54-8
1,2,4,5-Tetrafluorobenzene

: 603-35-0
triphenylphosphine

: 176174-70-2
1,4-bis(diphenylphosphino)-2,5-difluorobenzene

Guidance literature:: With lithium; ammonium chloride; Yield given. Multistep reaction; 1.) THF, overnight then 3 h, 2.) THF, 90 min, addition and 2 h;
DOI:10.1039/DT9960001077

Reference yield: 83.0%

: 59967-36-1,65337-26-0
cis-tetracarbonylbis(piperidine)molybdenum

: 176174-70-2
1,4-bis(diphenylphosphino)-2,5-difluorobenzene

: 5112-95-8
bis(diphenylphosphino)acetylene

: [(Mo(CO)4)2(C₂₆H₂₀P₂)(C₃₀H₂₂F₂P₂)]*CH₂Cl₂

Guidance literature:: In dichloromethane; stirring (room temp., 50 min); removal of volatiles (reduced pressure), washing (light petroleum), crystn. (CH2Cl2/MeOH); elem. anal.;
DOI:10.1039/DT9960001077