CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

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Chemical Name:CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄
CAS No.:131611-98-8
Molecular Formula:C₄₀H₆₁CoO₈P₄*ClO₄
Molecular Weight:952.258
Hs Code.:

CoH(P(OC<sub>2</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>5</sub>))4<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=CoH(P(OC<sub>2</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>5</sub>))4ClO<sub>4</sub>

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Chemical Property of CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

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Technology Process of CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

There total 1 articles about CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131629-82-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

: 131611-98-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1: Zn or NaBH₄ / not given

2: LiClO₄ / dichloromethane

With Zn or NaBH₄; LiClO₄; In dichloromethane;
DOI:10.1039/DT9900002979

Reference yield: 70.0%

: 131611-98-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

: 1885-81-0
p-chlorophenyl isocyanide

: 131612-02-7
Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆

Guidance literature:: With NaPF₆; In ethanol; dichloromethane; addn. of an excess of isocyanide to soln. of Co-compd. (under Ar, Schlenk app.) in CH2Cl2, cooling to -80°C, then warming to room temp., stirring for 20 min; solvent removal under reduced pressure, treating of residue with EtOH, then addn. of NaPF6 in EtOH, crystn. by slow cooling of its saturated soln. in EtOH at about 30-40°C, elem. anal.;
DOI:10.1039/DT9900002979