(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2

Base Information

Chemical Name:(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2
CAS No.:225116-14-3
Molecular Formula:C₃₃H₃₃MoP₂S₂
Molecular Weight:651.645
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Mo(SCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

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Chemical Property of (C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2

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Technology Process of (C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2

There total 4 articles about (C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.88%

: 225116-07-4
(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Cl^(1-) = [(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2]Cl

: 225116-14-3
(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2

Guidance literature:: With t-BuOK; In tetrahydrofuran; (N2); addn. of t-BuOK to a suspension of Mo complex in THF, stirring (room temp., 24 h); solvent removal (vac.), extn. (toluene), filtration (Celite), evapn. (reduced pressure), washing (cold pentane), drying (vac.); elem. anal.;
DOI:10.1039/a809903k

Reference yield: 55.0%

: molybdenum(cyclopentadienyl)Cl₂

: 3190-79-2
(2-mercaptoethyl)diphenylphosphine

: 225116-14-3
(C₅H₅)Mo(SCH₂CH₂P(C₆H₅)2)2

Guidance literature:: With MeLi; In tetrahydrofuran; (N2); addn. of MeLi to the org. ligand in THF, addn. of this soln. to a suspension of Mo complex in THF, stirring (room temp., overnight); evapn. (reduced pressure); extn. (toluene), filtration (Celite), evapn. (vac.), washing (cold pentane), drying (vac.);
DOI:10.1039/a809903k