(fluorenone)tricarbonylchromium⁽⁰⁾

Base Information

Chemical Name:(fluorenone)tricarbonylchromium⁽⁰⁾
CAS No.:69056-30-0
Molecular Formula:C₁₆H₈CrO₄
Molecular Weight:316.233
Hs Code.:

(fluorenone)tricarbonylchromium<sup>(0)</sup>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (fluorenone)tricarbonylchromium⁽⁰⁾

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Technology Process of (fluorenone)tricarbonylchromium⁽⁰⁾

There total 1 articles about (fluorenone)tricarbonylchromium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 69056-32-2,69056-33-3,33635-16-4
(η(6)-fluorene)chromiumtricarbonyl

: 80937-33-3
oxygen

: 86-73-7
9H-fluorene

: 486-25-9,952573-42-1
9-fluorenone

: 38980-16-4,69056-30-0,69056-31-1
(fluorenone)tricarbonylchromium⁽⁰⁾

Guidance literature:: In N,N-dimethyl-formamide; Electrochem. Process; electrochemical generation of O2(1-) from O2 supplied to the cathode compartment (H-cell, DMF, supporting electrolyte (C4H9)4NPF6); pouring catholyte (with excess O2(1-)) into a flask containing flourene; bubbling O2, 10min, dark;; diln. of catholyte with H2O; extn. with diethyl ether; drying; removal of solvent, vac.; column chromy. (silica gel; eluent: hexane/CH2Cl2 (50%));;
DOI:10.1016/0022-328X(84)80546-X