1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

Base Information

Chemical Name:1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose
CAS No.:652990-22-2
Molecular Formula:C₅₄H₅₈O₉S₂
Molecular Weight:915.181
Hs Code.:

Synonyms:

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Chemical Property of 1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

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Technology Process of 1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

There total 3 articles about 1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 652990-21-1
1',2,3,3',4,4'-hexa-O-benzyl-6,6'-di-O-mesylsucrose

: 1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-disulfidosucrose

: 1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-sulfidosucrose

: 652990-22-2
1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

Guidance literature:: With sodium hydrogensulfide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1081/CAR-120026473

Reference yield:

: 392699-44-4
6-O-acetyl-1,3,4-tri-O-benzyl-β-D-fructofuranosyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 652990-22-2
1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / MeONa / methanol / 0.5 h / 20 °C

2: 84 percent / Et₃N / CH₂Cl₂ / 1 h / 20 °C

3: 43 percent / NaHS*nH₂O / dimethylformamide / 1 h / 20 °C

With sodium hydrogensulfide; sodium methylate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120026473

Reference yield:

: 74761-34-5
1’,2,3,3’,4,4’-hexa-O-benzylsucrose

: 652990-22-2
1',2,3,3',4,4'-hexa-O-benzyl-6,6'-dideoxy-6,6'-dithiosucrose

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Et₃N / CH₂Cl₂ / 1 h / 20 °C

2: 43 percent / NaHS*nH₂O / dimethylformamide / 1 h / 20 °C

With sodium hydrogensulfide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120026473