((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂

Base Information

Chemical Name:((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂
CAS No.:157998-40-8
Molecular Formula:C₃₁H₃₃Cl₂OPRu
Molecular Weight:624.552
Hs Code.:

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>3</sub>)((C<sub>6</sub>H<sub>5</sub>)2PCH(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C(O)CH<sub>3</sub>)RuCl<sub>2</sub>

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Chemical Property of ((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂

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Technology Process of ((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂

There total 1 articles about ((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 52462-31-4
[RuCl2(η(6)-1,3,5-C6H3Me3)]2

: 16247-25-9
Diphenyl-(3-oxo-1-phenylbutyl)-phosphin

: 157998-40-8
((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂

Guidance literature:: In dichloromethane; under inert gas, stirring for 2 days; removing solvent (vac.), extn. of residue (hot toluene/CH2Cl2), filtn.,covering filtrate with hexane, elem. anal.;

Reference yield: 56.0%

: ammonium hexafluorophosphate

: 157998-40-8
((CH₃)3C₆H₃)((C₆H₅)2PCH(C₆H₅)CH₂C(O)CH₃)RuCl₂

: (C₉H₁₂)((C₆H₅)2PCH(C₆H₅)CH₂C(CH₃)O)RuCl⁽¹⁺⁾*PF₆^(1-)*0.5CH₂Cl₂=[(C₉H₁₂)((C₁₂H₁₀)PCH(C₆H₅)CH₂C(CH₃)O)RuCl]PF₆*0.5CH₂Cl₂

Guidance literature:: In methanol; dichloromethane; dissolving Ru-complex and NH4PF6 in CH2Cl2, addn. of methanol, heating at reflux overnight; evapn. (vac.), extn. of residue (CH2Cl2), filtn., covering with Et2O, elem. anal.;