((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane

Base Information

• Chemical Name: ((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane
• CAS No.: 1196795-87-5
• Molecular Formula: C₅H₁₂*C₇₂H₉₀Bi₄Br₆O₈
• Molecular Weight: 2471
• Mol file: 1196795-87-5.mol

Synonyms:

Chemical Property of ((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane

There total 1 articles about ((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

tris(bis(trimethylsilyl)amido)bismuth + 4-bromopropofol (2432-03-3) + pentane (109-66-0,8031-35-4,9078-70-0) → ((4-Br-2,6-iPr2C6H4O)2Bi(μ3-O)Bi(μ2-O-4-Br-2-iPr-6-[(C=CH2)CH2]C6H2-1:2κ2O,2κC))2*pentane (1196795-87-5) + Bi(O-2,6-iPr2-4-BrC6H2)3

Guidance literature:

In pentane; (N2) soln. phenol in pentane was added to soln. Bi(N(SiMe3)2)3 in pentane and stirred for 12 h; ppt. was filtered out, washed with pentane and dried in vacuo; elem. anal.;

DOI:10.1021/ic901134t

upstream raw materials:

4-bromopropofol

pentane