N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl

Base Information

• Chemical Name: N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl
• CAS No.: 890133-57-0
• Molecular Formula: C₁₅H₂₉AlN₂Si₂
• Molecular Weight: 320.561
• Mol file: 890133-57-0.mol

Synonyms:

Chemical Property of N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl

Chemical Property:

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Useful:

Technology Process of N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl

There total 1 articles about N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

N,N,N'-tris(trimethylsilyl)benzamidine (24261-90-3) + trimethylaluminum (75-24-1) → N,N'-bis(trimethylsilyl)benzamidinate aluminum dimethyl (890133-57-0)

Guidance literature:

In benzene; byproducts: SiMe4; under inert conditions; benzamidine suspended in dry hexane; cooled to -78°C; AlMe3 in hexane added dropwise; warmed to room temp.; stirred for 3 h; concd. by vac.; hexane removed partially; filtered; ppt. dried under vac.; elem. anal.;

DOI:10.1021/om0602198

upstream raw materials:

N,N,N'-tris(trimethylsilyl)benzamidine

trimethylaluminum