[1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron

Base Information

Chemical Name:[1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron
CAS No.:106906-04-1
Molecular Formula:C₂₉H₂₈Cl₂FeO₂P₂Si
Molecular Weight:625.326
Hs Code.:

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Chemical Property of [1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron

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Technology Process of [1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron

There total 2 articles about [1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 97374-34-0
tetracarbonyl(dichloromethylsilyl)hydridoiron

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 38894-55-2,14881-58-4
1,2-bis(diphenylphosphino)ethaneiron(0) tricarbonyl

: 106906-04-1
[1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron

Guidance literature:: In benzene; addn. of ligand to the Fe compd. in benzene under N2 and stirring at room temp. for 2 h; evapn. (vac.), extn. with petroleum ether, recrystn. from CH2Cl2/petroleum ether (2 times); elem. anal.;

Reference yield:

: 58894-89-6
[bis(dichloromethylsilyl)tetracarbonyliron]

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 38894-55-2,14881-58-4
1,2-bis(diphenylphosphino)ethaneiron(0) tricarbonyl

: 14977-13-0,39022-97-4
(CO)4Fe(C₆H₅)2PCH₂CH₂P(C₆H₅)2Fe(CO)4

: 106906-02-9
mer-μ-[1,2-bis(diphenylphosphino)ethane]-bis[tricarbonylbis(dichloromethylsilyl)iron]

: 106906-12-1
[1,2-bis(diphenylphosphino)ethane]-trans-dicarbonyl-cis-bis(dichloromethylsilyl)iron

: 106906-04-1
[1,2-bis(diphenylphosphino)ethane]dicarbonyl(dichloromethylsilyl)hydridoiron

Guidance literature:: In benzene; byproducts: (Cl2(CH3)Si)2O; stirring at 60°C under N2 for 3 days; filtration and evapn. (vac.); identification of product mixt. by IR andNMR;