tetraphenylstibonium azide

Base Information

Chemical Name:tetraphenylstibonium azide
CAS No.:24696-68-2
Molecular Formula:C₂₄H₂₀N₃Sb
Molecular Weight:472.193
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylstibonium azide

Chemical Property:

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Technology Process of tetraphenylstibonium azide

There total 1 articles about tetraphenylstibonium azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19638-17-6,16894-68-1
tetraphenylantimony(V) chloride

: 24696-68-2,36573-10-1
tetraphenylstibonium azide

Guidance literature:: With N₃-loaded Amberjet 4200 resin; In ethanol; water; 2:1 H2O:EtOH, soln. was passed out the resin; resin was washed with H2O until no ppt. with AgNO3, eluent was pumped off;
DOI:10.1002/zaac.200500289

Reference yield: 60.0%

: 24696-68-2,36573-10-1
tetraphenylantimony(V) azide

: 103-72-0
phenyl isothiocyanate

: 1-phenyl-4-(tetraphenylantimony) tetrazole-5-thione

Guidance literature:: In neat (no solvent); warming a mixt. of equimol. amts. of the Sb- and S-compds. to 90-100°C on a water bath for 4 h; recrystn. of the viscous liq. obtained from hexane; elem. anal.;