cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6

Base Information

• Chemical Name: cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6
• CAS No.: 1233766-64-7
• Molecular Formula: C₂₄H₂₁F₂N₄OPtS*F₆P
• Molecular Weight: 791.564
• Mol file: 1233766-64-7.mol

Synonyms:

Chemical Property of cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6

There total 1 articles about cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

ammonium hexafluorophosphate + dichloro(1,10-phenanthroline)platinum(II) (18432-95-6) + N-(diethylcarbamothioyl)-2,6-difluorobenzamide (1196586-76-1) → cis-[Pt(κ2S,O-2,6-F2C6H3C(O)NC(S)NEt2)(1,10-phenanthroline)]PF6 (1233766-64-7)

Guidance literature:

In acetonitrile; mixt. of Pt-complex, ligand, NH4PF6 in MeCN and N(CH2CH3)2 or NaCH3CO2 refluxed; concd. in vacuo, H2O added, filtered, washed with H2O, Et2O, dried in vac.;

DOI:10.1016/j.poly.2010.03.010

upstream raw materials:

dichloro(1,10-phenanthroline)platinum(II)

N-(diethylcarbamothioyl)-2,6-difluorobenzamide

Refernces