[WCl₃(NC₁₀H₇)(PMePh₂)2]

Base Information

Chemical Name:[WCl₃(NC₁₀H₇)(PMePh₂)2]
CAS No.:330433-93-7
Molecular Formula:C₃₆H₃₃Cl₃NP₂W
Molecular Weight:831.821
Hs Code.:

[WCl<sub>3</sub>(NC<sub>10</sub>H<sub>7</sub>)(PMePh<sub>2</sub>)2]

Synonyms:

Suppliers and Price of [WCl₃(NC₁₀H₇)(PMePh₂)2]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [WCl₃(NC₁₀H₇)(PMePh₂)2]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [WCl₃(NC₁₀H₇)(PMePh₂)2]

There total 1 articles about [WCl₃(NC₁₀H₇)(PMePh₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: W⁽⁶⁺⁾*4Cl^(1-)*NC₁₀H₇^(2-)=[WCl₄(NC₁₀H₇)]

: 1486-28-8
diphenyl(methyl)phosphine

: 330433-93-7
[WCl₃(NC₁₀H₇)(PMePh₂)2]

Guidance literature:: With sodium-mercury amalgam; In benzene; (N2); addn. of suspn. of (WCl4(NC10H7))2 (1 equiv.) in benzene to sodium-mercury amalgam (2 equiv. of Na) under benzene and PMePh2 (4 equiv.) using cannula; stirring for 2 h; filtration, removal of solvent, recrystn. from CH2Cl2 and light petroleum; elem. anal.;
DOI:10.1039/b006420n

Reference yield: 89.0%

: 330433-93-7
[WCl₃(NC₁₀H₇)(PMePh₂)2]

: 672-66-2
Dimethyl(phenyl)phosphine

: 330433-97-1
[WCl₂(NC₁₀H₇)(PMe₂Ph)3]

Guidance literature:: With sodium-mercury amalgam; In benzene; (N2); addn. of suspn. of (WCl3(NC10H7)(PMe2Ph)2) (1.1 mmol) in benzene to sodium-mercury amalgam (1.2 mmol of Na) under benzene and PMe2Ph (1.1 mmol) using cannula; stirring for 14 h; filtration twice, removal of solvent, recrystn. from mixt. of CH2Cl2 andlight petroleum; elem. anal.;
DOI:10.1039/b006420n